Research Article
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Year 2019, , 29 - 42, 30.06.2019

Saliha Cetinyokus , Meltem Dogan , Nesli Kucuktepe

https://doi.org/10.29002/asujse.527882

Abstract

References

  • [1] N. Pomerantz, Y.H. Ma, Journal of Membrane Science, 370 (2011) 97-108.
  • [2] A.M. Tarditi, F. Braun, M.İ. Cornaglia, Applied Surface Science, 257 (2011) 6626-6635.
  • [3] A. Goldbach, L. Yuan, H. Xu, Seperation and Purification Technology, 73 (2010) 65-70.
  • [4] A.D. Fontana, N. Sirini, L.M. Cornaglia, A.M. Tarditi, Journal of Membrane Science 563 (2018) 351–359.
  • [5] J. Melendez, N. Nooijer, K. Coenen, E. Fernandez, J.L. Viviente, M.S. Annaland, P.L. Arias, D.A.P. Tanaka, F. Gallucci, Journal of Membrane Science, 542 (2017) 329–341.
  • [6] K. Lee, M. Yuan, J. Wilcox, The Journal of Physical Chemistry, 119 (2015) 19642-19653
  • [7] C.H. Kim, J.Y. Han, N.C. Kim, S.K. Ryi, D.W. Kim, Journal of Membrane Science, 502 (2016) 57-64.
  • [8] N.S. Patki, S.T.B. Lundin, J.D. Way, Separation and Purification Technology, 191 (2018) 370–374.
  • [9] I.P. Mardilovich, B. Castro-Dominguez, N.K. Kazantzis, T. Wu, Y.H. Ma, International Journal of Hydrogen Energy, 40 (2015) 6107-6117.
  • [10] H. Lu, L. Zhu, W. Wang, W. Yang, J. Tang, International Journal of Hydrogen Energy, 40 (2015) 3548-3556.
  • [11] H.W. Abu El Hawa, S.N. Paglieri, C.C. Morris, A. Harale, J.D. Way, Journal of Membrane Science, 466 (2014)151-160.
  • [12] V.N. Alimov, A.O. Busnyuk, M.E. Notkin, E.Y. Peredistov, A.I. Livshits, Journal of Membrane Science, 481 (2015) 54-62.
  • [13] V.N. Alimova, I.V. Bobylevb, A.O. Busnyuka, M.E. Notkina, E.Y. Peredistova, A.I. Livshitsa, Journal of Membrane Science, 549 (2018) 428–437.
  • [14] T.B. Flanagan, D. Wang, Journal of Alloys and Compounds, 767 (2018) 1264-1270.
  • [15] E. Yan, H. Huang, R. Min, P. Zhao, R. D.K. Misra, P. Huang, F. Xu, L. Sun, International Journal of Hydrogene Energy, 43 (2018) 14466- 14477.
  • [16] J.H. Lee, J.Y. Han, K.M. Kim, S.K. Ryi, D.W. Kim, Journal of Membrane Science, 492 (2015) 242-248.
  • [17] T.A. Peters, M. Stange, P. Veenstra, A. Nijmeijer, A. Bredesen, Journal of Membrane Science, 499 (2016) 105-115.
  • [18] R.J. Westerwaal, E.A. Bouman, W.G. Haije, H. Schreuders, S. Dutta, M.Y. Wu, C. Boelsma, P. Ngene, S. Basak, B. Dam, International Journal of Hydrogen Energy, 40 (2015) 3932 -3943.
  • [19] N.A. Al-Mufachi, N.V. Rees, R. Steinberger-Wilkens, Renewable and Sustainable Energy Reviews, 47 (2015) 540-551.
  • [20] S. Nayebossari, J. Speight, D. Book, Journal of Membrane Science, 451 (2014) 216-225.
  • [21] M.S. Islam, M.M. Rahman, S. Ilias, International Journal of Hydrogen Energy, 37 (2012) 3477-3490.
  • [22] H. Gao, Y.S. Lin, Y. Li, B. Zhang, Journal of Membrane Science, 265 (2005) 142-152.
  • [23] H. Lim, T.S. Oyama, Journal of Membrane Science, 378 (2011) 179-185.
  • [24] L. Yuan, A. Goldbach, H. Xu, Journal of Membrane Science, 322 (2008) 39-45.

Effects of Synthesis Conditions on the PdCu Membrane Structure

Year 2019, , 29 - 42, 30.06.2019

Saliha Cetinyokus , Meltem Dogan , Nesli Kucuktepe

https://doi.org/10.29002/asujse.527882

Abstract

In this study, it was aimed to plate PdCu alloy layer
on porous glass supports by using electroless plating technique. It was also
aimed to achieve coexistence of fcc (face-centered cubic) and bcc
(body-centered cubic) phases on the alloy membrane layer. The fcc and bcc
phases were seen together in the structures of the membranes synthesized at all
three bath temperatures (30 °C, 40 °C and 50 °C), but, it was shown that the
most suitable coating rate was achieved when the coating bath temperature was
40 °C. The appropriate composition of PdCu (74% Pd, 26% Cu) was achieved by
following a synthesis procedure as follows: Coating in Pd bath three times for
60 minutes each followed by coating in Cu bath at the low formaldehyde
concentration (5 mL/L) for 15 minutes. Hydrogen flux in the membrane was
measured as 1.9x10-6 mol/cm2s. After flux measurements,
it was determined that the membrane structure changed and the fcc (200)
structure, which did not previously exist in the structure, was formed.

Keywords

Electroless plating PdCu Composite membrane Characterization

References

  • [1] N. Pomerantz, Y.H. Ma, Journal of Membrane Science, 370 (2011) 97-108.
  • [2] A.M. Tarditi, F. Braun, M.İ. Cornaglia, Applied Surface Science, 257 (2011) 6626-6635.
  • [3] A. Goldbach, L. Yuan, H. Xu, Seperation and Purification Technology, 73 (2010) 65-70.
  • [4] A.D. Fontana, N. Sirini, L.M. Cornaglia, A.M. Tarditi, Journal of Membrane Science 563 (2018) 351–359.
  • [5] J. Melendez, N. Nooijer, K. Coenen, E. Fernandez, J.L. Viviente, M.S. Annaland, P.L. Arias, D.A.P. Tanaka, F. Gallucci, Journal of Membrane Science, 542 (2017) 329–341.
  • [6] K. Lee, M. Yuan, J. Wilcox, The Journal of Physical Chemistry, 119 (2015) 19642-19653
  • [7] C.H. Kim, J.Y. Han, N.C. Kim, S.K. Ryi, D.W. Kim, Journal of Membrane Science, 502 (2016) 57-64.
  • [8] N.S. Patki, S.T.B. Lundin, J.D. Way, Separation and Purification Technology, 191 (2018) 370–374.
  • [9] I.P. Mardilovich, B. Castro-Dominguez, N.K. Kazantzis, T. Wu, Y.H. Ma, International Journal of Hydrogen Energy, 40 (2015) 6107-6117.
  • [10] H. Lu, L. Zhu, W. Wang, W. Yang, J. Tang, International Journal of Hydrogen Energy, 40 (2015) 3548-3556.
  • [11] H.W. Abu El Hawa, S.N. Paglieri, C.C. Morris, A. Harale, J.D. Way, Journal of Membrane Science, 466 (2014)151-160.
  • [12] V.N. Alimov, A.O. Busnyuk, M.E. Notkin, E.Y. Peredistov, A.I. Livshits, Journal of Membrane Science, 481 (2015) 54-62.
  • [13] V.N. Alimova, I.V. Bobylevb, A.O. Busnyuka, M.E. Notkina, E.Y. Peredistova, A.I. Livshitsa, Journal of Membrane Science, 549 (2018) 428–437.
  • [14] T.B. Flanagan, D. Wang, Journal of Alloys and Compounds, 767 (2018) 1264-1270.
  • [15] E. Yan, H. Huang, R. Min, P. Zhao, R. D.K. Misra, P. Huang, F. Xu, L. Sun, International Journal of Hydrogene Energy, 43 (2018) 14466- 14477.
  • [16] J.H. Lee, J.Y. Han, K.M. Kim, S.K. Ryi, D.W. Kim, Journal of Membrane Science, 492 (2015) 242-248.
  • [17] T.A. Peters, M. Stange, P. Veenstra, A. Nijmeijer, A. Bredesen, Journal of Membrane Science, 499 (2016) 105-115.
  • [18] R.J. Westerwaal, E.A. Bouman, W.G. Haije, H. Schreuders, S. Dutta, M.Y. Wu, C. Boelsma, P. Ngene, S. Basak, B. Dam, International Journal of Hydrogen Energy, 40 (2015) 3932 -3943.
  • [19] N.A. Al-Mufachi, N.V. Rees, R. Steinberger-Wilkens, Renewable and Sustainable Energy Reviews, 47 (2015) 540-551.
  • [20] S. Nayebossari, J. Speight, D. Book, Journal of Membrane Science, 451 (2014) 216-225.
  • [21] M.S. Islam, M.M. Rahman, S. Ilias, International Journal of Hydrogen Energy, 37 (2012) 3477-3490.
  • [22] H. Gao, Y.S. Lin, Y. Li, B. Zhang, Journal of Membrane Science, 265 (2005) 142-152.
  • [23] H. Lim, T.S. Oyama, Journal of Membrane Science, 378 (2011) 179-185.
  • [24] L. Yuan, A. Goldbach, H. Xu, Journal of Membrane Science, 322 (2008) 39-45.
There are 24 citations in total.

Details

Primary Language English
Subjects Engineering
Journal Section Research Article
Authors

Saliha Cetinyokus 0000-0001-9955-6428

Meltem Dogan

Nesli Kucuktepe

Publication Date June 30, 2019
Submission Date February 15, 2019
Acceptance Date May 27, 2019
Published in Issue Year 2019

Cite

APA Cetinyokus, S., Dogan, M., & Kucuktepe, N. (2019). Effects of Synthesis Conditions on the PdCu Membrane Structure. Aksaray University Journal of Science and Engineering, 3(1), 29-42. https://doi.org/10.29002/asujse.527882
Aksaray J. Sci. Eng. | e-ISSN: 2587-1277 | Period: Biannually | Founded: 2017 | Publisher: Aksaray University | https://asujse.aksaray.edu.tr