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Year 2018, Volume: 2 Issue: 2, 25 - 37, 28.12.2018

Abstract

References

  • [1]. Aksoy, S, & Ruzgar, S. (2015). Effect of Nitrogen on optical properties of ZnO film deposited by sol gel method. J Mater Electron Dev, 1, 33-37. [2]. Arif, B. (2015). Determination of optical constants of ZnO growth by PECVD Method. J Mater Electron Dev, 1, 28-32. [3]. Arif, Bilal, El-Nasser, HM, Dere, A, Al-Ghamdi, Ahmed A, Bin-Omran, S, El-Tantawy, Farid, & Yakuphanoglu, F. (2015). Optical properties of Zn1− xAlxO: NiO transparent metal oxide composite thin films prepared by sol–gel method. Journal of Sol-Gel Science and Technology, 76(2), 378-385. [4]. Biroo, Safiye Jameel, Canbay, Canan AKSU, Aziz, Sivar, & Özkul, İskender. (2018). Structural properties of CdO-ZnO Semiconductor Composite. Paper presented at the 1st International Engineering and Technology Symposium, Batman. [5]. Biroo, Safiye Jameel, Canbay, Canan AKSU, Ünlü, Nihan, & Özkul, İskender. (2018). Optical properties of ZnO-3CdO Synthesized by Hydrothermal Method. Paper presented at the 1st International Engineering and Technology Symposium, Batman. [6]. Caglar, M, & Yakuphanoglu, F. (2012). Structural and optical properties of copper doped ZnO films derived by sol–gel. Applied Surface Science, 258(7), 3039-3044. [7]. Caglar, Mujdat, Ilican, Saliha, Caglar, Yasemin, & Yakuphanoglu, Fahrettin. (2009). Electrical conductivity and optical properties of ZnO nanostructured thin film. Applied surface science, 255(8), 4491-4496. [8]. Chandiramouli, R, & Jeyaprakash, BG. (2013). Review of CdO thin films. Solid State Sciences, 16, 102-110. [9]. El-Nahass, MM, Farag, AAM, & Atta, AA. (2009). Influence of heat treatment and gamma-rays irradiation on the structural and optical characterizations of nano-crystalline cobalt phthalocyanine thin films. Synthetic Metals, 159(7), 589-594. [10]. Guan, Rongfa, Kang, Tianshu, Lu, Fei, Zhang, Zhiguo, Shen, Haitao, & Liu, Mingqi. (2012). Cytotoxicity, oxidative stress, and genotoxicity in human hepatocyte and embryonic kidney cells exposed to ZnO nanoparticles. Nanoscale research letters, 7(1), 602. [11]. Hasim, Siti Nuurul Fatimah, Hamid, Muhammad Azmi Abdul, Shamsudin, Roslinda, & Jalar, Azman. (2009). Synthesis and characterization of ZnO thin films by thermal evaporation. Journal of Physics and Chemistry of Solids, 70(12), 1501-1504. [12]. Jayaraman, Vinoth Kumar, Kuwabara, Yasuhiro Matsumoto, & Álvarez, Arturo Maldonado. (2016). Importance of substrate rotation speed on the growth of homogeneous ZnO thin films by reactive sputtering. Materials Letters, 169, 1-4. [13]. Jule, Leta T, Dejene, Francis B, Ali, Abdub G, Roro, Kittessa T, Hegazy, Aiat, Allam, Nageh K, & El Shenawy, Essam. (2016). Wide visible emission and narrowing band gap in Cd-doped ZnO nanopowders synthesized via sol-gel route. Journal of Alloys and Compounds, 687, 920-926. [14]. Karthik, K, Dhanuskodi, S, Gobinath, C, & Sivaramakrishnan, S. (2015). Microwave-assisted synthesis of CdO–ZnO nanocomposite and its antibacterial activity against human pathogens. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy, 139, 7-12. [15]. Kim, Jong Hun, Hong, Yong Cheol, & Uhm, Han Sup. (2007a). Binary oxide material made from a mixture of Zn and Cd in a microwave plasma. Chemical physics letters, 443(1), 122-126. [16]. Kim, Jong Hun, Hong, Yong Cheol, & Uhm, Han Sup. (2007b). Synthesis of oxide nanoparticles via microwave plasma decomposition of initial materials. Surface and Coatings Technology, 201(9), 5114-5120. [17]. Kumar, P Senthil, Selvakumar, M, Bhagabati, Purabi, Bharathi, B, Karuthapandian, S, & Balakumar, S. (2014). CdO/ZnO nanohybrids: facile synthesis and morphologically enhanced photocatalytic performance. Rsc Advances, 4(62), 32977-32986. [18]. Lehraki, N, Aida, MS, Abed, S, Attaf, N, Attaf, A, & Poulain, Marcel. (2012). ZnO thin films deposition by spray pyrolysis: influence of precursor solution properties. Current Applied Physics, 12(5), 1283-1287. [19]. Li, Guangming, Wang, Xinchang, Wang, Yinghua, Shi, Xinwei, Yao, Ning, & Zhang, Binglin. (2008). Synthesis and field emission properties of ZnCdO hollow micro–nano spheres. Physica E: Low-dimensional Systems and Nanostructures, 40(8), 2649-2653. [20]. Lv, Yuzhen, Guo, Lin, Xu, Hubin, & Chu, Xiangfeng. (2007). Gas-sensing properties of well-crystalline ZnO nanorods grown by a simple route. Physica E: Low-dimensional Systems and Nanostructures, 36(1), 102-105. [21]. Mahmoud, Waleed E, & Al-Ghamdi, AA. (2010). Synthesis of CdZnO thin film as a potential candidate for optical switches. Optics & Laser Technology, 42(7), 1134-1138. [22]. Margan, Payam, & Haghighi, Mohammad. (2018). Sono-coprecipitation synthesis and physicochemical characterization of CdO-ZnO nanophotocatalyst for removal of acid orange 7 from wastewater. Ultrasonics Sonochemistry, 40, 323-332. [23]. Martellucci, Sergio, Chester, Arthur N, & Mignani, Anna Grazia. (2002). Optical Sensors and Microsystems. New York, Boston, London. [24]. Ocakoglu, K, Mansour, Sh A, Yildirimcan, S, Al-Ghamdi, Ahmed A, El-Tantawy, F, & Yakuphanoglu, F. (2015). Microwave-assisted hydrothermal synthesis and characterization of ZnO nanorods. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy, 148, 362-368. [25]. Rana, N, Chand, Subhash, & Gathania, Arvind K. (2015). Tailoring the structural and optical properties of ZnO by doping with Cd. Ceramics International, 41(9), 12032-12037. [26]. Saravanan, R, Gracia, F, Khan, Mohammad Mansoob, Poornima, V, Gupta, Vinod Kumar, Narayanan, V, & Stephen, A. (2015). ZnO/CdO nanocomposites for textile effluent degradation and electrochemical detection. Journal of Molecular Liquids, 209, 374-380. [27]. Shan, CX, Liu, Z, Zhang, ZZ, Shen, DZ, & Hark, SK. (2006). A simple route to porous ZnO and ZnCdO nanowires. The Journal of Physical Chemistry B, 110(23), 11176-11179. [28]. Wang, Wei-Wei, & Zhu, Ying-Jie. (2004). Shape-controlled synthesis of zinc oxide by microwave heating using an imidazolium salt. Inorganic Chemistry Communications, 7(9), 1003-1005. [29]. Xian, Fenglin, Miao, Kaibo, Bai, Xuecheng, Ji, Yun, Chen, Feier, & Li, Xiangyin. (2013). Characteraction of Ag-doped ZnO thin film synthesized by sol–gel method and its using in thin film solar cells. Optik-International Journal for Light and Electron Optics, 124(21), 4876-4879.

The Hydrothermal Synthesis of ZnO-CdO Composite and Physical and Electrical Characterization

Year 2018, Volume: 2 Issue: 2, 25 - 37, 28.12.2018

Abstract

In this study, ZnO-CdO composites were synthesized by hydrothermal
method. Two different contents of the nano-composites have been fabricated for
the investigation of structural, morphological, optical and electrical
properties. X-ray diffraction (XRD), FTIR, scanning electron microscopy (SEM),
UV-VIS-NIR spectrophotometer and two probe methods were used for these analyses.
At the same time, the chemical analysis of the sample was measured by EDX
analysis. The TG-DTA analyses were made to determine the thermal stability. The
optical band gap of composites was found to be 2.78 and 3.06 eV, respectively,
with an increase in the content of the Zn precursor.

References

  • [1]. Aksoy, S, & Ruzgar, S. (2015). Effect of Nitrogen on optical properties of ZnO film deposited by sol gel method. J Mater Electron Dev, 1, 33-37. [2]. Arif, B. (2015). Determination of optical constants of ZnO growth by PECVD Method. J Mater Electron Dev, 1, 28-32. [3]. Arif, Bilal, El-Nasser, HM, Dere, A, Al-Ghamdi, Ahmed A, Bin-Omran, S, El-Tantawy, Farid, & Yakuphanoglu, F. (2015). Optical properties of Zn1− xAlxO: NiO transparent metal oxide composite thin films prepared by sol–gel method. Journal of Sol-Gel Science and Technology, 76(2), 378-385. [4]. Biroo, Safiye Jameel, Canbay, Canan AKSU, Aziz, Sivar, & Özkul, İskender. (2018). Structural properties of CdO-ZnO Semiconductor Composite. Paper presented at the 1st International Engineering and Technology Symposium, Batman. [5]. Biroo, Safiye Jameel, Canbay, Canan AKSU, Ünlü, Nihan, & Özkul, İskender. (2018). Optical properties of ZnO-3CdO Synthesized by Hydrothermal Method. Paper presented at the 1st International Engineering and Technology Symposium, Batman. [6]. Caglar, M, & Yakuphanoglu, F. (2012). Structural and optical properties of copper doped ZnO films derived by sol–gel. Applied Surface Science, 258(7), 3039-3044. [7]. Caglar, Mujdat, Ilican, Saliha, Caglar, Yasemin, & Yakuphanoglu, Fahrettin. (2009). Electrical conductivity and optical properties of ZnO nanostructured thin film. Applied surface science, 255(8), 4491-4496. [8]. Chandiramouli, R, & Jeyaprakash, BG. (2013). Review of CdO thin films. Solid State Sciences, 16, 102-110. [9]. El-Nahass, MM, Farag, AAM, & Atta, AA. (2009). Influence of heat treatment and gamma-rays irradiation on the structural and optical characterizations of nano-crystalline cobalt phthalocyanine thin films. Synthetic Metals, 159(7), 589-594. [10]. Guan, Rongfa, Kang, Tianshu, Lu, Fei, Zhang, Zhiguo, Shen, Haitao, & Liu, Mingqi. (2012). Cytotoxicity, oxidative stress, and genotoxicity in human hepatocyte and embryonic kidney cells exposed to ZnO nanoparticles. Nanoscale research letters, 7(1), 602. [11]. Hasim, Siti Nuurul Fatimah, Hamid, Muhammad Azmi Abdul, Shamsudin, Roslinda, & Jalar, Azman. (2009). Synthesis and characterization of ZnO thin films by thermal evaporation. Journal of Physics and Chemistry of Solids, 70(12), 1501-1504. [12]. Jayaraman, Vinoth Kumar, Kuwabara, Yasuhiro Matsumoto, & Álvarez, Arturo Maldonado. (2016). Importance of substrate rotation speed on the growth of homogeneous ZnO thin films by reactive sputtering. Materials Letters, 169, 1-4. [13]. Jule, Leta T, Dejene, Francis B, Ali, Abdub G, Roro, Kittessa T, Hegazy, Aiat, Allam, Nageh K, & El Shenawy, Essam. (2016). Wide visible emission and narrowing band gap in Cd-doped ZnO nanopowders synthesized via sol-gel route. Journal of Alloys and Compounds, 687, 920-926. [14]. Karthik, K, Dhanuskodi, S, Gobinath, C, & Sivaramakrishnan, S. (2015). Microwave-assisted synthesis of CdO–ZnO nanocomposite and its antibacterial activity against human pathogens. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy, 139, 7-12. [15]. Kim, Jong Hun, Hong, Yong Cheol, & Uhm, Han Sup. (2007a). Binary oxide material made from a mixture of Zn and Cd in a microwave plasma. Chemical physics letters, 443(1), 122-126. [16]. Kim, Jong Hun, Hong, Yong Cheol, & Uhm, Han Sup. (2007b). Synthesis of oxide nanoparticles via microwave plasma decomposition of initial materials. Surface and Coatings Technology, 201(9), 5114-5120. [17]. Kumar, P Senthil, Selvakumar, M, Bhagabati, Purabi, Bharathi, B, Karuthapandian, S, & Balakumar, S. (2014). CdO/ZnO nanohybrids: facile synthesis and morphologically enhanced photocatalytic performance. Rsc Advances, 4(62), 32977-32986. [18]. Lehraki, N, Aida, MS, Abed, S, Attaf, N, Attaf, A, & Poulain, Marcel. (2012). ZnO thin films deposition by spray pyrolysis: influence of precursor solution properties. Current Applied Physics, 12(5), 1283-1287. [19]. Li, Guangming, Wang, Xinchang, Wang, Yinghua, Shi, Xinwei, Yao, Ning, & Zhang, Binglin. (2008). Synthesis and field emission properties of ZnCdO hollow micro–nano spheres. Physica E: Low-dimensional Systems and Nanostructures, 40(8), 2649-2653. [20]. Lv, Yuzhen, Guo, Lin, Xu, Hubin, & Chu, Xiangfeng. (2007). Gas-sensing properties of well-crystalline ZnO nanorods grown by a simple route. Physica E: Low-dimensional Systems and Nanostructures, 36(1), 102-105. [21]. Mahmoud, Waleed E, & Al-Ghamdi, AA. (2010). Synthesis of CdZnO thin film as a potential candidate for optical switches. Optics & Laser Technology, 42(7), 1134-1138. [22]. Margan, Payam, & Haghighi, Mohammad. (2018). Sono-coprecipitation synthesis and physicochemical characterization of CdO-ZnO nanophotocatalyst for removal of acid orange 7 from wastewater. Ultrasonics Sonochemistry, 40, 323-332. [23]. Martellucci, Sergio, Chester, Arthur N, & Mignani, Anna Grazia. (2002). Optical Sensors and Microsystems. New York, Boston, London. [24]. Ocakoglu, K, Mansour, Sh A, Yildirimcan, S, Al-Ghamdi, Ahmed A, El-Tantawy, F, & Yakuphanoglu, F. (2015). Microwave-assisted hydrothermal synthesis and characterization of ZnO nanorods. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy, 148, 362-368. [25]. Rana, N, Chand, Subhash, & Gathania, Arvind K. (2015). Tailoring the structural and optical properties of ZnO by doping with Cd. Ceramics International, 41(9), 12032-12037. [26]. Saravanan, R, Gracia, F, Khan, Mohammad Mansoob, Poornima, V, Gupta, Vinod Kumar, Narayanan, V, & Stephen, A. (2015). ZnO/CdO nanocomposites for textile effluent degradation and electrochemical detection. Journal of Molecular Liquids, 209, 374-380. [27]. Shan, CX, Liu, Z, Zhang, ZZ, Shen, DZ, & Hark, SK. (2006). A simple route to porous ZnO and ZnCdO nanowires. The Journal of Physical Chemistry B, 110(23), 11176-11179. [28]. Wang, Wei-Wei, & Zhu, Ying-Jie. (2004). Shape-controlled synthesis of zinc oxide by microwave heating using an imidazolium salt. Inorganic Chemistry Communications, 7(9), 1003-1005. [29]. Xian, Fenglin, Miao, Kaibo, Bai, Xuecheng, Ji, Yun, Chen, Feier, & Li, Xiangyin. (2013). Characteraction of Ag-doped ZnO thin film synthesized by sol–gel method and its using in thin film solar cells. Optik-International Journal for Light and Electron Optics, 124(21), 4876-4879.
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Details

Primary Language English
Subjects Engineering
Journal Section Articles
Authors

Canan Aksu Canbay 0000-0002-5151-4576

Safiye Jameel Biro This is me

İskender Özkul

Publication Date December 28, 2018
Published in Issue Year 2018 Volume: 2 Issue: 2

Cite

APA Aksu Canbay, C., Biro, S. J., & Özkul, İ. (2018). The Hydrothermal Synthesis of ZnO-CdO Composite and Physical and Electrical Characterization. Journal of Engineering and Technology, 2(2), 25-37.